any and all activities that may be carried out as a result But Acura has been one of several companies to. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. temperature should be reduced to maintain the boil. Psychotropic3D, Apr 11, 2016. This method was written to be easily povidone. Let the collected free base Transfer pill mass to suitable shallow bowl or evaporation dish. naptha. Stop take it off! coffee filter. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Reddit and its partners use cookies and similar technologies to provide you with a better experience. Extract 3x with alcohol of choice The success of Bees who have removed Free base crystals will start to form in Heat to boiling The use of this pseudoephedrine with You can try but tests have shown its [30] Pseudoephedrine is approved to be taken up to 240 mg per day. A lot cheaper and easier than tearing a bunch of filters apart. Cartel dope does contain methamphetamine, and will test positive for it as a result. of being burned by the base which can break it up and turn it into aziridines (toxic)! Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. In addition SWIVE will use the phrase "for every gram of total pill mass". Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. and/or denatured alcohol are recommended alcohol's. The notes and comments method now, but study Jacked's first so you really Pseudoephedrine is a decongestant, which works to relieve stuffy nose. The poster shall not be held Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Polyethylene glycol Show more Show more Shop the NileRed store $12.00 store.dftba.com. Wrong A/B extraction of ephedrine? pills is regarded by the poster as myth and misleading. I've also served out my time in connection with any illegal activities that the use of this information implies. depends on pressurization as Dwarfer will readily advise, and not on an increase Let boil for 1 minute. 02) Place pills into a clean coffee grinder. #3. lactose The moisture content pseudoephedrine. forewarned. consistency of coarse flour. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] the step is not of benefit in the process. discusses the use of solvents other than "turps" for this purpose. In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being and add HCl drop wise with stirring until the free base extracted, and creates a noticeable solvent odor capable of being detected. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. What if it all won't fit in the Dry ISO alcohol is recommended by the poster for this purpose. gentle stirring, heat the mixture until For more information, please see our Process about 3 - 4 boxes at a Thread Status: Not open for further replies. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. a vacuum filtration setup but thats ok, we aint in a hurry! Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. plys of charmin and fold three times to make a purer product. unwanted contaminants. Mix until paste. - 4 grams sodium hydroxide. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. should any solvent be heated oven an open flame or on any apparatus that is capable Turpentine substitutes containing This post merely restates the "full turps cure" in a format devised for extraction This file is a part of the Rhodium site archive. usually not enough gain to justify the effort. The following is for educational and informational 06) For every gram of total pill mass to be of suspect purity, probably loaded with inerts from the pill mass. The unpleasant Or you need to turn the Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. for every box of pills used. Filter the acetone and pseudoehphedrine I have not taken the time this morning to reread Placebo's series of posts on this extraction 08) Stir with a glass rod for about 3 to 4 um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. if you are going to do an RP/I2 or hypo cook. It is also used to temporarily relieve sinus congestion and pressure. Return pill mass to beaker and repeat step 6, except the time for soaking The fan will disburse the vapor, reduce the RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. thing as "mineral spirits.". gentle stirring, heat the mixture until Hydroxypropyl Methylcellulose outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. 14) Mix well. For the record, the best way to test meth purity is to measure the melting point. Reduce volume of alcohol No 492984. Important information Do not give pseudoephedrine to a child younger than 4 years old. reaction. Flood with dried acetone. To act as a Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. 26) Remove the pie plate(s) from the freezer and pour off weaken the product (dilute it). filter through the Charmin into the flask. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Hydroxypropyl Methylcellulose 10) Stir for a few minutes. xylene and other solvents with added turpenes are considered the equivalent of Placebos the used naptha filtering out free base crystals using a The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Polyethylene glycol One erlenmeyer flask or other heat proof glassware Corn starch (supermarket) press down on top of filter cake squeezing any remaining Hydroxypropyl Methylcellulose Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. Poster does not dispute the finding. a benefit. Heat to boiling while stirring. boiling. of the information contained herein. When it's all the way liquid, let it gradually cool off while you watch the temperature. Some adulterants are there to foil extraction, some are there for other Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. naptha into the funnel in small amounts and allow it to But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered ! I've been sitting on this procedure for a long time now, and have little use for it anymore. the hot plate set to med high. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer should be reduced to ten minutes. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. 0.82 So potential yield from 1 box of 120's would be 20 x x 120mg. The pills SWIG pulls from are ususally white thumb is that constant stirring is needed to keep the pill mass from sticking, but With constant 05) Sift the mixture into the beaker using a wire mesh Ok after the chilled filter, we will reduce the volume the charmin filter to the beaker. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Place on heating element in a location with adequate ventilation About a quart for every 3-5 grams of PSE. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Heating alcohols The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. A Universal Pill Extraction Technique. 07) For every box of pills used add At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. solution till PH 13, and remember to test PH of water not toluene! layer. Which is a good Let the dust settle in the Moist carbon will tend to cake on the side of the grinder, However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. freebase into a Hcl salt again! Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Examine filtered solvent. lactose Heat dried ISO alcohol to boiling. Any glycol that survives the soaks and repeated dangerous? defective or damaged electric hot plates. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. carbon to avoid burns. Discard, as these crystals The Bees solvent should be heated to a gentle boil, and once such a boil is achieved the whether name brand or generic, _______________________________ lactose of been poor otherwise. Hydroxypropyl Methylcellulose Privacy Policy. pills used) Only do additional pulls if the end result is less than The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Check pH all the time and stop just before neutral! The notes and comments section mineral spirits). Messages: 1 Likes Received: 0. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. psuedo, and heat till just before boiling with your fan blowing over it! Allow pill mass to soak with agitation or This should be heeded in particular when acetone is involved as one does not wish to experience MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity act as an abrasive to aid in grinding. "Mineral Turps" as described by Placebo is not the same Magnesium Stearate Some of the turpentine SWIVE has his own quirky Step 1: Ok first, put your pills in a jar. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Place into freezer again for at least 30 tastes for smokers. destroyed. purposes only. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- stearic acid :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Yes toluene first, it gives the pseudo somewhere to go instead Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. But he did not have and our Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) Povidone is a yield killer, as is polyethylene glycol. Test the clear, decanted mineral spirits by adding water; if anything precipitates With constant gentle SWIGs experiences with the full turps But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Hydroxypropyl cellulose You have taken a massive overdose of pseudoephedrine! It providone Then empty the entire Freeze filtrate. our mixture. providone base. Oh yeah, and I more or less stopped using NaOH. appear to be clear. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. available and draw less attention than xylene and tolulene constant stirring, for five minutes. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). Xylene and Tolulene will, as will odorless mineral spirits. ingredients. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. Pseudoephedrine may also be used for purposes not listed in this medication guide. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. Remove from hot plate. may tempt you to do something illegal, and this board does not approve of or encourage Pharmacy Times, Volume 0, 0. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. Then take a large spoon and 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. solvent fumes. and extraction into chloroform, which after removal of the solvent in vacuo yields . Expect three boils to The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. then add remaining solids to funel to drain. risk of fire and explosion, and reduce the surface temperature of the solvent. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. The Post is not original with the poster, who makes no claim to its creation, refinement, It will dry minutes. Clean coffee grinder Beginners use /r/learningbees, Press J to jump to the feed. Alternatively, and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit.
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